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Synthesis of hydroxyapatite through solid-state reaction method and study of its thermoluminesence dosimetric properties against gamma rays

عنوان مقاله: Synthesis of hydroxyapatite through solid-state reaction method and study of its thermoluminesence dosimetric properties against gamma rays
شناسه ملی مقاله: JR_RPE-3-2_002
منتشر شده در در سال 1401
مشخصات نویسندگان مقاله:

Parisa Taghipour - Department of Physics‎, ‎Faculty of Sciences‎, ‎University of Mohaghegh Ardabili‎, ‎P.O‎. ‎Box ۱۷۹‎, ‎Ardabil‎, ‎Iran
Farhad Zolfagharpour - Department of Physics‎, ‎Faculty of Sciences‎, ‎University of Mohaghegh Ardabili‎, ‎P.O‎. ‎Box ۱۷۹‎, ‎Ardabil‎, ‎Iran
Hamideh Daneshvar - Radiation Application Research School‎, ‎Nuclear Science & Technology Research Institute‎, ‎P.O‎. ‎Box ۱۱۳۶۵-۳۴۸۶‎, ‎Tehran‎, ‎Iran

خلاصه مقاله:
In this research work, powder hydroxyapatite samples were synthesized using a solid-state reaction method to investigate the annealing effect. The crystal structure was carried out by XRD system produced data, and the Rietveld method using MAUD software. The samples were irradiated in different radiation absorbed doses up to ۱۵۰۰Gy and their thermoluminescence properties including glow curve, response, fading effect and reproducibility were investigated from dosimetry point of view. The results showed that the annealing temperature significantly affects the crystal structure and thermoluminescence dosimetry response of hydroxyapatite samples, consequently. It was concluded that high temperature annealing process can lead to formation of β-TCP crystal phase during the synthesis of hydroxyapatite. Percentage of this formed phase increases with rising the temperature, and finally leads to increasing of the thermoluminescence response. It was concludded that in the solid state reaction method to increasing the TL response, it is better to use high annealing temperature for the synthesis of hydroxyapatite sample.

کلمات کلیدی:
Hydroxyapatite, Solid state, Thermoluminescence, Dosimetry, Rietveld refinement

صفحه اختصاصی مقاله و دریافت فایل کامل: https://civilica.com/doc/1451093/