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Preconcentration of Copper Ion on Modified Magnetic Fe3O4@SiO2 Nanoparticles in some Environmental Samples and its Determination by Electrothermal Atomic Absorption Spectrometry

عنوان مقاله: Preconcentration of Copper Ion on Modified Magnetic Fe3O4@SiO2 Nanoparticles in some Environmental Samples and its Determination by Electrothermal Atomic Absorption Spectrometry
شناسه ملی مقاله: JR_IJEE-7-4_006
منتشر شده در شماره 4 دوره 7 فصل در سال 1395
مشخصات نویسندگان مقاله:

m Naghizadeh - Department of Chemistry, Shahid Bahonar University of Kerman, Kerman, Iran /Shahid Bahonar University of Kerman, Kerman, Iran
m.a Taher - Department of Chemistry, Shahid Bahonar University of Kerman, Kerman, Iran
m Behzadi - Department of Chemistry, Shahid Bahonar University of Kerman, Kerman, Iran
f Hassani Moghaddam - Department of Chemistry, Shahid Bahonar University of Kerman, Kerman, Iran /Shahid Bahonar University of Kerman, Kerman, Iran

خلاصه مقاله:
Magnetic silica nanoparticles modified by 3-[2-(2-aminoethylamino) ethylamino] propyltrimethoxysilane (AAAPTS) and Salicylaldehyde were prepared and used as a new adsorbent for extraction and preconentration of copper ion through magnetic solid-phase extraction (MSPE) method.After adsorption, these ions were desorbed with nitric acid followed by the determination with electrothermal atomic absorption spectrometry. Fourier transform infrared spectroscopy (FT-IR), fieldemission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD) spectrometry and vibrating sample magnetometer (VSM) were used to characterize the adsorbent. The MSPE conditions were optimized

کلمات کلیدی:
Magnetic solid-phase extraction,Silica nanoparticles,Salicylaldehyde,Determination of copper,

صفحه اختصاصی مقاله و دریافت فایل کامل: https://civilica.com/doc/630441/