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The effects of solvent and ultrasonic irradiation in synthesis of novel supramolecular compound

عنوان مقاله: The effects of solvent and ultrasonic irradiation in synthesis of novel supramolecular compound
شناسه ملی مقاله: IICC20_016
منتشر شده در بیستمین سمینار شیمی معدنی ایران در سال 1397
مشخصات نویسندگان مقاله:

Bagher souri - Department of chemistry, University of Sistan and Baluchestan,P. O. Box ۹۸۱۳۵-۶۷۴, Zahedan, Iran
Soheila abbasi - Department of chemistry, University of Sistan and Baluchestan,P. O. Box ۹۸۱۳۵-۶۷۴, Zahedan, Iran
Alireza Rezvani - Department of chemistry, University of Sistan and Baluchestan,P. O. Box ۹۸۱۳۵-۶۷۴, Zahedan, Iran

خلاصه مقاله:
coordination compounds are very interesting because of their interesting properties such as: sensing, catalysis, separation, gas storage, lasers, transistors [1-3]. One cadmium(II) zero-dimensional supra molecule compound [Cd(L)2(I)2] (1), {L= 2-picolyl amin} has been synthesized by branch tube and sonochemical irradiation methods. In order to study the effects of solvent and time of reaction on the formation of [Cd(L)2(I)2] (1) supra molecule compound, some experiments were designed and four samples of 1 were synthesized by sonochemical process. Less time of reaction resulted in the formation of smaller particles with mix morphologies. These micro and nano crystals were characterized by IR spectroscopy, X-ray powder diffraction (XRD) and Scanning Electron Microscopy (SEM).

کلمات کلیدی:
Morphology, Sonochemical process., branch tube method.

صفحه اختصاصی مقاله و دریافت فایل کامل: https://civilica.com/doc/876317/