Effect of graphite addition on the microstructure, mechanical properties and oxidation resistance of HfB۲-SiC composites prepared by the SPS method
محل انتشار: ماهنامه بین المللی مهندسی، دوره: 35، شماره: 10
سال انتشار: 1401
نوع سند: مقاله ژورنالی
زبان: انگلیسی
مشاهده: 183
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شناسه ملی سند علمی:
JR_IJE-35-10_002
تاریخ نمایه سازی: 15 تیر 1401
چکیده مقاله:
Among the intermediate metal diborides, HfB۲ and ZrB۲ are the most suitable options for high temperature applications. Compounds such as borides, carbides and nitrides of the IV-V group intermediate metals, which have melting temperatures above ۳۰۰۰ °C [۱], are known as ultra high temperature ceramics (UHTCs). In this study, HfB۲-SiC-graphite composites have been fabricated using spark plasma sintering at ۱۹۰۰ ℃ for ۱۰ min. The effect of graphite content on microstructure, mechanical properties were studied and also oxidation resistance of prepared composites was investigated at ۱۴۰۰ ℃ for ۳۲ h. Weight changes and the thickness of formed oxide layer was measured. The relative density, toughness and strength of SPSed composites were increased with inccraesing of graphite up ۲.۵ wt% and then decraesed. The hardness of composites were decreased when graphite was added. The oxidation resistance of composite improved after graphite addition up ۲.۵ wt%, while ecessive quantity of graphite caused to poor oxidation resistance of composite.
کلیدواژه ها:
HfB۲-SiC composite ، Spark plasma sintering (SPS) ، ultra-high temperature ceramic (UHTC) ، oxidation ، Graphite
نویسندگان
mohammad sakvand
Faculty of Chemical and Materials Engineering, Shahrood University of Technology, Shahrood, Iran
maryam shojaei
chemical and materials engineering department-shahrood university of technology
leila nikzad
Department of Ceramic, Materials and Energy Research Center, Karaj, Iran