Performance of glucose, sucrose and cellulose as carbonaceous precursors for the synthesis of B۴C powders
محل انتشار: فصلنامه سنتز و تفجوشی، دوره: 2، شماره: 1
سال انتشار: 1401
نوع سند: مقاله ژورنالی
زبان: انگلیسی
مشاهده: 68
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شناسه ملی سند علمی:
JR_SYNSINT-2-1_005
تاریخ نمایه سازی: 14 آذر 1402
چکیده مقاله:
Boron carbide is the third hardest material in the world after diamond and cubic boron nitride, which is one of the most strategic engineering ceramics in various industrial applications. The aim of this research is to synthesize B۴C by reacting boric acid as boron source with polymers from the saccharide family as carbon sources, and to determine the best saccharide as precursor. For this purpose, glucose (monosaccharide), sucrose (disaccharide), and cellulose (polysaccharide) were used and examined. The samples were prepared by appropriate mixing of the starting materials, pyrolysis at ۷۰۰ °C, and synthesis at ۱۵۰۰ °C. The results of Fourier transform infrared (FT-IR) spectroscopy and X-ray diffractometry (XRD) showed that among the studied saccharide polymers, glucose is the best carbon source candidate for the synthesis of B۴C. To describe precisely, the specimen prepared with glucose and boric acid had more boron carbide and less hydrocarbon.
کلیدواژه ها:
نویسندگان
Seyed Faridaddin Feiz
Ceramics Department, Materials and Energy Research Center (MERC), Karaj, Iran
Leila Nikzad
Ceramics Department, Materials and Energy Research Center (MERC), Karaj, Iran
Hudsa Majidian
Ceramics Department, Materials and Energy Research Center (MERC), Karaj, Iran
Esmaeil Salehi
Ceramics Department, Materials and Energy Research Center (MERC), Karaj, Iran