Sol-gel Approach for the Synthesis and Characterization of Mg and Cu Substituted Mn-Zn Ferrite Nanoparticles

سال انتشار: 1402
نوع سند: مقاله ژورنالی
زبان: انگلیسی
مشاهده: 20

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شناسه ملی سند علمی:

JR_IJMSEI-21-1_006

تاریخ نمایه سازی: 28 اسفند 1402

چکیده مقاله:

The Mn-Zn ferrite with a composition of Mn۰.۲۵Mg۰.۰۸Cu۰.۲۵Zn۰.۴۲Fe۲O۴ has been synthesized in this study using the chemical sol-gel technique at a pH of ۷. The sample was prepared and subsequently annealed at a temperature of ۷۰۰°C. The nanocrystalline ferrite samples were subjected to characterization using X-ray diffraction (XRD), Fourier transform-infrared spectroscopy (FT-IR), Scanning electron microscopy (SEM), Thermogravimetry (TG), and Differential thermal analysis (DTA). The findings of these observations are delineated and deliberated. The sample's phase composition was verified using X-ray diffraction examination. The crystalline size was determined using Scherrer's formula and was observed to be within the range of ۲۰-۷۵ nm. Two notable stretching bands were seen in the FTIR spectra within the range of ۴۰۰-۶۵۰ cm-۱. The spinel structure of the produced nanoparticles was confirmed by these two bands. The magnetic characteristics of the powder were examined using a Vibrating Sample Magnetometer (VSM). The presence of M-H hysteresis loops suggests that the produced nanoparticles have superparamagnetic properties, as evidenced by their low coercive force, remanent magnetization, and saturation magnetization values.

نویسندگان

Amit Bandekar

University of Mumbai, Maharashtra, India

Pravin Tirmali

Application Specialist, I.R. Technology Services Pvt. Ltd., Navi Mumbai Maharashtra, India

Paresh Gaikar

Department of Physics, Rayat Shikshan Sanstha’s, Karmaveer Bhaurao Patil College, Vashi, Maharashtra, India

Shriniwas Kulkarni

Department of Physics, The Institute of Science, Mumbai, Maharashtra, India

Nana pradhan

Department of Physics, The Institute of Science, Mumbai, Maharashtra, India

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