Ferric and Ferrous Molar ratio Effect on Physical and Magnetic Properties of Iron Oxide Nanoparticles

سال انتشار: 1402
نوع سند: مقاله ژورنالی
زبان: انگلیسی
مشاهده: 22

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شناسه ملی سند علمی:

JR_IJMSEI-21-1_002

تاریخ نمایه سازی: 28 اسفند 1402

چکیده مقاله:

Iron oxide nanoparticles has attracted extensively due to their supermagnetic properties, preferred in biomedicine because of their biocompatibility and potential nontoxicity to human beings. Synthesis of iron nanoparticles (FeNPs) was prepared with the help of ferric chloride and ferrous sulphate by using the coprecipitation method. The variation and combination of ferric and ferrous concentrations affect the physical and magnetic properties of iron oxide nanoparticles.  The effect of ۰.۱ M ferric and ferrous concentration on iron oxide nanoparticles studied separately and in combination. The obtained nanoparticles were characterized by Particle size, zeta potential, Ultraviolet (UV-visible), Fourier Transform Infrared Spectroscopy (FTIR), X-ray diffraction (XRD), Scanning electron microscope (SEM), Thermal gravimetric analysis (TGA), and Vibrating-sample magnetometer (VSM) techniques. Particle size was below ۲۰۰nm and zeta potential was within the limit for all the batches. UV visible spectra at ۲۲۴ nm, and FTIR exhibit two peaks at ۵۱۰ and ۵۹۴ cm-۱, indicating iron oxide NPs and XRD confirmed the crystalline nature of Fe. SEM showed a spherical shape for all batches. The use of a combination of ferric and ferrous is more effective than its individual use. TGA and VSM studies confirmed its magnetic properties.

نویسندگان

Amruta Patil

Department of Pharmaceutical Chemistry, Dr. D. Y. Patil College of Pharmacy, Akurdi, Pune ۴۱۱۰۴۴, India

Sonali Mahaparale

Department of Pharmaceutical Chemistry, Dr. D. Y. Patil College of Pharmacy, Akurdi, Pune ۴۱۱۰۴۴, India

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